Golden Gate In-situ Reaction Cell ATR

The Golden Gate in-situ reaction cell allows in compartment reaction monitoring over a broad range of extreme conditions.

 

Description

Golden Gate | In-situ Reaction Cell ATR

The In-Situ Reaction Cell for the Golden Gate ATR is used for monitoring processes in a heated and pressurised reactor by single-reflection ATR spectroscopy. A stirring mechanism is an optional add-on.

Features

  • Pressurised reaction cell: The 24 ml cell can be pressurised to 3000 psi and heated to 200 °C. It features a cooling jacket and has 1/8th inch Swagelok fittings for in-flow of reactants.
  • Resistant materials: The In-Situ reaction chamber can be manufactured from Stainless-Steel or Haselloy, depending on the application. The monolithic diamond ATR crystal is robust and chemically resistant.
  • Optional stirring device: A motorised variable speed stirrer with sapphire shaft and integrated pressure cap is available as an option.

The Golden Gate uses focusing lenses to achieve a tightly focused beam on the diamond ATR crystal. The standard lens material is ZnSe but KRS-5 lenses are also available as an option where access to the lower wavenumber region of the spectrum is required.

Specifications

ATR crystal Monolithic diamond
Crystal sealing The diamond is sealed with a metal braze into a tungsten puck.
Angle of incidence 45o
Spectral range ZnSe lenses 5000-700 cm-1 KRS-5 lenses 6500-400 cm-1
Temperature range Ambient to 200 oC
Pressure range Ambient to 3000 psi
Fittings 1/8th Swagelok
Cell material Stainless-Steel or Hastelloy

 

Datasheet

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